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Flux growth at ambient pressure of millimeter-sized single crystals of LaFeAsO, LaFeAsO1−xFx, and LaFe1−xCoxAsO
Applied Physics Letters
  • J.-Q. Yan, Iowa State University
  • Shibabrata Nandi, Iowa State University
  • Jerel L. Zarestky, Iowa State University
  • W. Tian, Iowa State University
  • Andreas Kreyssig, Iowa State University
  • Brandt A. Jensen, Iowa State University
  • A. Kracher, Iowa State University
  • Kevin W. Dennis, Iowa State University
  • Robert J. McQueeney, Iowa State University
  • Alan I. Goldman, Iowa State University
  • R. William McCallum, Iowa State University
  • Thomas A. Lograsso, Iowa State University
Document Type
Article
Publication Date
12-3-2009
DOI
10.1063/1.3268435
Abstract

Millimeter-sized single crystals of LaFeAsO, LaFeAsO1−xFx, and LaFe1−xCoxAsO were grown in NaAs flux at ambient pressure. The detailed growth procedure and crystal characterizations are reported. The as-grown crystals have typical dimensions of3×4×0.05–0.3 mm3 with the crystallographic c-axis perpendicular to the plane of the platelike single crystals. Various characterizations confirmed the high quality of our LaFeAsO crystals. Co and F were introduced into the lattice leading to superconductingLaFe1−xCoxAsO and LaFeAsO1−xFx single crystals, respectively. This growth protocol is expected to be broadly applicable to grow other RMAsO (R = rare earth, M = transitionmetal) compounds.

Comments

The following article appeared in Applied Physics Letters 95 (2009): 222504 and may be found at http://dx.doi.org/10.1063/1.3268435.

Rights
Copyright 2009 American Institute of Physics. This article may be downloaded for personal use only. Any other use requires prior permission of the author and the American Institute of Physics.
Copyright Owner
American Institute of Physics
Language
en
File Format
application/pdf
Citation Information
J.-Q. Yan, Shibabrata Nandi, Jerel L. Zarestky, W. Tian, et al.. "Flux growth at ambient pressure of millimeter-sized single crystals of LaFeAsO, LaFeAsO1−xFx, and LaFe1−xCoxAsO" Applied Physics Letters Vol. 95 Iss. 22 (2009) p. 222504
Available at: http://works.bepress.com/thomas_lograsso/136/