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Presentation
Processing Of Al-Cu-Fe Single Grains
Ames Laboratory Conference Papers, Posters, and Presentations
  • Thomas A. Lograsso, Iowa State University
  • A. R. Ross, Iowa State University
  • Dwight W. Delaney, Motorola, Inc.
Document Type
Conference Proceeding
Disciplines
Conference
MRS Fall Meeting & Exhibit
Publication Date
1-1-1998
DOI
10.1557/PROC-553-3
Abstract

The phase equilibria of the Al-Cu-Fe quasicrystalline phase (y phase) is complex and conventional crystal growth techniques like the Bridgman and Czochralski methods are not applicable in preparation of large crystals. Large single grains of the y phase been have prepared by either slow cooling or isothermal anneals. In the later technique, arc melted ingots were subjected to either single or multiple heat treatments between 825 and 840°C to encourage grain growth. Following heat treatment, grains of the icosahedral phase are found either as isolated pentagonal-faceted crystals within the ingot or within clusters of intergrown grains. The growth of the large grains is independent of the sample processing history of the sample, is facilitated by the presence of liquid at the growth temperatures and is constrained by the physical dimension of the ingot. The microstructure of both grain types is similar containing a minor quantity (on the order of 5–10 %) of a second phase and a high degree of porosity in the as-grown state. The second phase is usually present as a thin layer between adjacent grains or associated with a pore within a single grain. The grain porosity is distributed throughout the ingot. These defects can be removed through post-growth hot isostatic pressing and anneal treatments.

Comments

This article is from MRS Proceedings 553 (1998): 3–12, doi:10.1557/PROC-553-3.

Copyright Owner
Materials Research Society
Language
en
Citation Information
Thomas A. Lograsso, A. R. Ross and Dwight W. Delaney. "Processing Of Al-Cu-Fe Single Grains" Boston, MA(1998)
Available at: http://works.bepress.com/thomas_lograsso/128/