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Article
High-speed photographic study of vaporclouds from wet droplets and the subsequent solid particles in an inductively coupled plasma
Ames Laboratory Accepted Manuscripts
  • Christopher H. Ebert, Iowa State University and Ames Laboratory
  • Nathan J. Saetveit, Iowa State University and Ames Laboratory
  • Stanley J. Bajic, Iowa State University and Ames Laboratory
  • Daniel S. Zamzow, Iowa State University and Ames Laboratory
  • David P. Baldwin, Iowa State University and Ames Laboratory
  • Robert S. Houk, Iowa State University and Ames Laboratory
Publication Date
6-17-2020
Department
Ames Laboratory; Chemistry
OSTI ID+
1634871
Report Number
IS-J 10244
DOI
10.1039/D0JA00210K
Journal Title
Journal of Analytical Atomic Spectrometry
Abstract

Movies of an inductively coupled plasma (ICP) while nebulizing a concentrated sample of yttrium were recorded using a high-speed camera with short exposure time (10 μs) and fast framing rate (5000 frames per s). Clouds from large droplets can be seen in several successive frames as they travel downstream in the axial channel of the ICP. These droplet clouds are superimposed on the usual spatial structure of red YO, neutral Y atom and blue Y+ emission. As a particular large droplet moves downstream, its red emission cloud evolves into a faint white streak with a surrounding cloud of blue Y+ emission. The streak is attributed to a solid residue from the droplet. The velocity of the droplet and subsequent particle is measured to be 28 m s−1. The general characteristics of the droplet and particle clouds agree well with previous photographic measurements and those by other methods such as laser induced-fluorescence or scattering.

DOE Contract Number(s)
AC02-07CH11358
Language
en
Publisher
Iowa State University Digital Repository, Ames IA (United States)
Disciplines
Citation Information
Christopher H. Ebert, Nathan J. Saetveit, Stanley J. Bajic, Daniel S. Zamzow, et al.. "High-speed photographic study of vaporclouds from wet droplets and the subsequent solid particles in an inductively coupled plasma" Vol. 35 Iss. 9 (2020) p. 1956 - 1958
Available at: http://works.bepress.com/robert_houk/13/