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Article
Improvements in the synthesis and compaction of nanocrystalline materials
Nanostructured Materials (1998)
  • Paul G. Sanders, Argonne National Laboratory
  • G. E. Fougere, Argonne National Laboratory
  • L. J. Thompson, Argonne National Laboratory
  • J. A. Eastman, Argonne National Laboratory
  • J. R. Weertman, Northwestern University
Abstract
Processing defects such as porosity and impurities may be present in nanocrystalline materials produced by inert gas condensation and compaction. New synthesis and compaction devices were designed and built to improve the sample quality. Nanocrystalline Pd and Cu made in these new systems have reduced levels of hydrogen and oxygen impurities and increased density compared with materials made under similar conditions in the old system. It was more difficult to produce and maintain extremely fine grain sizes in the high-purity, high-density nanocrystalline Pd and Cu synthesized in this study.
Publication Date
May 19, 1998
DOI
10.1016/S0965-9773(97)00167-0
Publisher Statement
© 1997 Acta Metallurgica Inc. Publisher's version of record: https://doi.org/10.1016/S0965-9773(97)00167-0
Citation Information
Paul G. Sanders, G. E. Fougere, L. J. Thompson, J. A. Eastman, et al.. "Improvements in the synthesis and compaction of nanocrystalline materials" Nanostructured Materials Vol. 8 Iss. 3 (1998) p. 243 - 252 ISSN: 9780080914237
Available at: http://works.bepress.com/paul-sanders/42/