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Article
10,12-Dimethylpteridino[6,7-f][1,10]- phenanthroline-11,13(10H,12H)-dione– chloroform (1/1)
Acta Crystallographica Section E (2010)
  • Waynie Olaprath, Eastern Illinois University
  • Jennifer Rodin, Eastern Illinois University
  • Kraig A. Wheeler, Eastern Illinois University
  • Mark E. McGuire, Eastern Illinois University
Abstract

In the title co-crystal, C18H12N6O2_CHCl3, intramolecular Cl3C—H_ _ _N hydrogen-bonding interactions occur between a single CHCl3 and both N atoms at the 1,10-positions on the phenanthroline portion of the molecule. The interplanar distance between inversion-related molecules is 3.241 (2) A ° .

Keywords
  • single-crystal X-ray study,
  • T = 173 K,
  • mean _(C–C) = 0.002 A°,
  • R factor = 0.032,
  • wR factor = 0.095,
  • data-to-parameter ratio = 12.3
Disciplines
Publication Date
2010
Publisher Statement
The final version of this article is available open access via Acta Crystallographica Section E: http://journals.iucr.org/e/issues/2010/09/00/issconts.html doi:10.1107/S1600536810031570
Citation Information
Waynie Olaprath, Jennifer Rodin, Kraig A. Wheeler and Mark E. McGuire. "10,12-Dimethylpteridino[6,7-f][1,10]- phenanthroline-11,13(10H,12H)-dione– chloroform (1/1)" Acta Crystallographica Section E Vol. E66 Iss. 9 (2010)
Available at: http://works.bepress.com/kraig_wheeler/2/