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Article
Microstructural Characterization of Next Generation Nuclear Graphites
Microscopy and Microanalysis
  • Chinnathambi Karthik, Boise State University
  • Joshua Kane, Boise State University
  • Darryl P. Butt, Boise State University
  • William E. Windes, Center for Advanced Energy Studies
  • Rick Ubic, Boise State University
Document Type
Article
Publication Date
4-1-2012
Abstract

This article reports the microstructural characteristics of various petroleum and pitch based nuclear graphites (IG-110, NBG-18, and PCEA) that are of interest to the next generation nuclear plant program. Bright-field transmission electron microscopy imaging was used to identify and understand the different features constituting the microstructure of nuclear graphite such as the filler particles, microcracks, binder phase, rosette-shaped quinoline insoluble (QI) particles, chaotic structures, and turbostratic graphite phase. The dimensions of microcracks were found to vary from a few nanometers to tens of microns. Furthermore, the microcracks were found to be filled with amorphous carbon of unknown origin. The pitch coke based graphite (NBG-18) was found to contain higher concentration of binder phase constituting QI particles as well as chaotic structures. The turbostratic graphite, present in all of the grades, was identified through their elliptical diffraction patterns. The difference in the microstructure has been analyzed in view of their processing conditions.

Copyright Statement

This document was originally published by Cambridge University Press in Microscopy and Microanalysis. Copyright restrictions may apply. DOI: 10.1017/S1431927611012360

Citation Information
Chinnathambi Karthik, Joshua Kane, Darryl P. Butt, William E. Windes, et al.. "Microstructural Characterization of Next Generation Nuclear Graphites" Microscopy and Microanalysis (2012)
Available at: http://works.bepress.com/karthik_chinnathambi/8/