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Article
Neutron Irradiation Induced Microstructural Changes in NBG-18 and IG-110 Nuclear Graphites
Carbon
  • Chinnathambi Karthik, Boise State University
  • Joshua Kane, Boise State University
  • Darryl Butt, Boise State University
  • William E. Windes, Centre for Advanced Energy Studies
  • Rick Ubic, Boise State University
Document Type
Article
Publication Date
5-1-2015
Abstract
This paper reports the neutron-irradiation-induced effects on the microstructure of NBG-18 and IG-110 nuclear graphites. The high-temperature neutron irradiation at two different irradiation conditions was carried out at the Advanced Test Reactor National User Facility at the Idaho National Laboratory. NBG-18 samples were irradiated to 1.54 dpa and 6.78 dpa at 430 °C and 678 °C respectively. IG-110 samples were irradiated to 1.91 dpa and 6.70 dpa at 451 °C and 674 °C respectively. Bright-field transmission electron microscopy imaging was used to study the changes in different microstructural components such as filler particles, microcracks, binder and quinoline-insoluble (QI) particles. Significant changes have been observed in samples irradiated to about 6.7 dpa. The closing of pre-existing microcracks was observed in both the filler and the binder phases. The binder phase exhibited substantial densification with near complete elimination of the microcracks. The QI particles embedded in the binder phase exhibited a complete microstructural transformation from rosettes to highly crystalline solid spheres. The lattice images indicate the formation of edge dislocations as well as extended line defects bridging the adjacent basal planes. The positive climb of these dislocations has been identified as the main contributor to the irradiation-induced swelling of the graphite lattice.
Citation Information
Karthik, Chinnathambi; Kane, Joshua; Butt, Darryl P.; Windes, William E.; and Ubic, Rick. (2015). "Neutron Irradiation Induced Microstructural Changes in NBG-18 and IG-110 Nuclear Graphites". Carbon, 86, 124-131. doi: http://dx.doi.org/10.1016/j.carbon.2015.01.036