Polymeric nanocomposites imbedded with Multi-walled carbon nanotubes (MWNTs) are expected to have superior mechanical and electrical properties. However, these properties are achieved if uniform alignment and dispersion of MWNTs are attained. In mass production, achievement of these properties becomes a quality issue where it is necessary to control process parameters in order to achieve repeatability of the resultant nanocomposites properties.Therefore, this research will present the process design for the manufacturing of MWNTs-polymer nanocomposites using a thermoset and a thermoplastic polymers with the goal of achieving repeatable properties in a high volume production environment.