Article
Intragranular Nanocomposites via Internal Reduction of Carbide Solid Solutions
ECS Transactions
Abstract
A reaction-based processing technique to synthesize intragranularmetal-metal/carbide-matrix micro/nanocomposite particles via internal reduction of carbide solid solutions is introduced. The presented method is the first-demonstrated analogue of internal reduction in oxide solid solutions for non-oxide-based ceramic systems. Selected thermodynamic, kinetic, and crystallographic analyses are discussed.
Meeting Name
PRiME 2012 (2012: Oct. 7-12, Honolulu, HI)
Department(s)
Materials Science and Engineering
Keywords and Phrases
- Ceramic systems,
- Crystallographic analysis,
- Oxide solid solution,
- Processing technique, Solid solutions, Carbides
Document Type
Article - Conference proceedings
Document Version
Citation
File Type
text
Language(s)
English
Rights
© 2012 Electrochemical Society., All rights reserved.
Publication Date
10-1-2012
Publication Date
01 Oct 2012
Disciplines
Citation Information
David W. Lipke and Kenneth H. Sandhage. "Intragranular Nanocomposites via Internal Reduction of Carbide Solid Solutions" ECS Transactions Vol. 50 Iss. 44 (2012) p. 85 - 93 ISSN: 1938-5862; 1938-6737 Available at: http://works.bepress.com/david-lipke/4/
This work was supported by the U.S. Air Force Office of Scientific Research via Awards No. FA9550-07-1-0115 (supporting solid solution carbide syntheses, reaction experiments, and XRD and SEM analyses) and FA9550-09-1-0162 (supporting TEM/SAED analyses), and by the U.S. Department of Energy via Award No. DESC0002245 (supporting thermodynamic analyses).